The Maulide Group

Publications

2026

  • 230) Jakub Brześkiewicz, Kunj Kapur, Boris Maryasin, and Nuno Maulide*
    Deprotective Alkylation: A Platform for Alcohol-to-Amine Interconversion Using Nonafluoromesitylenesulfonamides
    Angewandte Chemie International Edition 2026, Early view, e3520541.
     
  • 229) Gwyndaf A. Oliver, Konstantin Günther, Chiara Sebastianelli-Schoditsch, Sophie Woolford, Iina Ludwig, Harald H. Sitte, and Nuno Maulide*
    Synthesis of Aminocyclopropanes by Redox-Neutral Aminoalkylation
    Angewandte Chemie International Edition 2026, Early view, e8092854.
    Press release: CeMM 2026
     
  • 228) Abigail W. Wilson, Giulianna A. Miseo, Christina A. Rivera, Neil K. Garg*, Jakob Frey#, Andreas Benedikt zur Bonsen#, and Nuno Maulide*#
    IBX-Mediated Amine Oxidation
    Organic Syntheses 2026, 103, 407-422.
    #As checkers. Since Volume 103, Organic Syntheses checkers are listed as co-authors.
     
  • 227) Jaehyun You, Donghyeon Kim, Yoonsu Park*, Eléonore Tacke#, Bjarne T. Schulz# and Nuno Maulide*#
    Preparation of 2-Iodoxybenzoic Acid (IBX)
    Organic Syntheses 2026, 103, 283-300.
    #As checkers. Since Volume 103, Organic Syntheses checkers are listed as co-authors.
     
  • 226) Angela K. Hofmeister, Giulia Iannelli, Péter Angyal, Augustin Malandain, Daniel Kaiser, Boris Maryasin, Hanspeter Kählig, Matteo Barel, Gaia Novarino and Nuno Maulide*
    Unified Synthesis of Unconventional α-Polyhalogenated Amines Through Hydroaminoalkylation
    Angewandte Chemie International Edition 2026, 65, e1233707.
     
  • 225) Uroš Vezonik, Giulia Iannelli, Daniel Kaiser and Nuno Maulide*
    An alkyl-swap platform for late-stage modification of secondary N-methylamines
    Nature Chemistry 2026, 18, 1650–1657.
    Highlighted in Synfacts 2026.
    Press release: University of Vienna 2026, MSN 2026, Phys.org 2026, Scienmag 2026, Bioengineer.org 2026.
     
  • 224) Konstantin Günther, Lorenz Erlbacher, Daniel Kaiser, Nuno Maulide*, Bryce M. Dye# and Richard E. Taylor*#
    Synthesis of 2-Oxo-2H-Pyran-3-yl Trifluoromethanesulfonate from Mucic Acid
    Organic Syntheses 2026, 103, 218–235.
    #As checkers. Since Volume 103, Organic Syntheses checkers are listed as co-authors.
     
  • 223) Marianna C. Tonoyan, Aimee K. Long, Neil K. Garg*, Milos Vavrik#, Nikolaos Skoulikas# and Nuno Maulide*#
    Preparation of 2-Iodoxybenzoic Acid (IBX)
    Organic Syntheses 2026, 103, 205–217.
    #As checkers. Since Volume 103, Organic Syntheses checkers are listed as co-authors.
     
  • 222) Philipp Spieß, Miloš Vavrík, Jakob Frey, Uroš Vezonik, Daniel Kaiser and Nuno Maulide*
    Cation Sampling Enables Regiodivergent Distal Functionalization of Ketones
    Journal of the American Chemical Society 2026, 148, 21230–21237.
    Press release: University of Vienna 2026, MSN 2026, Phys.org 2026, Chemie.de 2026, Miragenews 2026.
     
  • 221) Wen-Juan Yuan, Chao-Lai Tong, Feng-Ling Qing*, Uroš Vezonik#, Sabela Vega-Ces# and Nuno Maulide*#
    Copper-Mediated Oxidative Bromodifluoromethylation of Phenols:Preparation of Phenyl 4-(bromodifluoro-methoxy)benzoate
    Organic Syntheses 2026, 103, 192–204.
    #As checkers. Since Volume 103, Organic Syntheses checkers are listed as co-authors.
     
  • 220) Tim Schulte, Felix Waldbach, Tobias Ritter*, Kunj Kapur#, Daniya Aynetdinova# and Nuno Maulide*#
    Synthesis of Aryl Halides via a Safer Sandmeyer Reaction Protocol
    Organic Syntheses 2026, 103, 101–120.
    #As checkers. Since Volume 103, Organic Syntheses checkers are listed as co-authors.
     
  • 219) Iakovos Saridakis, Manuel Schupp, Haoqi Zhang, Thomas Leischner, Laura Marie Gail, Konstantin Günther, Martina Drescher, Florian Doubek, Daniel Kaiser, Georg Stary* and Nuno Maulide*
    Target-agnostic SAR mapping and immunological evaluation of (−)-FR252921 and analogs against primary human immune cells
    Chemical Science 2026, 17, 9912–9920.
     
  • 218) Alessio Di Ianni*, Thomas Fabian Leischner, Bogdan-Razvan Brutiu, Iakovos Saridakis, Andrea Di Ianni, Hendrik Krolle, Christian H. Ihling, Saad Shaaban, Nuno Maulide*, Andrea Sinz* and Claudio Iacobucci*
    Intrinsic N-Terminal Reactivity and Improved Analysis of DSSO-Carbamate and Carbamate-Based Cross-Linkers
    Analytical Chemistry 2026, 98, 8167–8178.

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2025

  • 217) Irmgard Tiefenbrunner, Saad Shaaban and Nuno Maulide*
    Deprotective Functionalization: An Emerging Concept for Amine Reactivity
    Chemistry – A European Journal 2025, 32, e03271.
     
  • 216) Daniya Aynetdinova, Jakub Brześkiewicz, Nikolaos Skoulikas and Nuno Maulide*
    Facile (Z)‐Selective Synthesis of β,γ‐Unsaturated Ketones by a Silicon‐based Olefination Strategy
    Angewandte Chemie International Edition 2025, 64, e202517069.
     
  • 215) Immo Klose, Christian Knittl-Frank, Nicolas G.-Simonian, Boris Maryasin, Daniel Kaiser and Nuno Maulide*
    Synthesis of Sterically Congested Carbonyl Compounds via an ipso-Selective Sulfonium Rearrangement
    Journal of the American Chemical Society 2025, 147, 37899–37906.
     
  • 214) Uroš Vezonik, Paolo Piacentini and Nuno Maulide*
    Acid-Mediated Hydroaminomethylation of Unactivated Alkenes
    Organic Syntheses 2025, 102, 414–427.
     
  • 213) Fränze Müller, Bogdan R. Brutiu, Iakovos Saridakis, Thomas Leischner, Micha J. Birklbauer, Manuel Matzinger, Mathias Madalinski, Thomas Lendl, Saad Shaaban, Viktoria Dorfer*, Nuno Maulide* and Karl Mechtler*
    Developing a new cleavable crosslinker reagent for in-cell crosslinking
    Communications Chemistry 2025, 8, 191.
     
  • 212) Giulia Iannelli, Philipp Spieß, Ricardo Meyrelles, Daniel Kaiser, Boris Maryasin, Leticia González* and Nuno Maulide*
    Diastereoselective Umpolung cyclisation of ketones promoted by hypervalent iodine
    Chemical Science 2025, 16, 10944–10950.
     
  • 211) Zhi-Jie Niu, Bogdan R. Brutiu, Margaux Riomet, Daniel Kaiser and Nuno Maulide*
    Charge Relocation Enables a Modular and Diastereoselective Synthesis of cis‐Substituted Tetrahydrofurans
    Angewandte Chemie International Edition 2025, 64, e202503750.
    Highlighted in Synfacts 2025.
     
  • 210) Oliver J. V. Belleza, Iakovos Saridakis, Nadja K. Singer, Xavier Westergaard, Sergio Armentia Matheu, Miran Lemmerer, Margaux Riomet, Pedro A. Sánchez-Murcia, Nina Kastner, Stefanie Rukavina, Yi Xiao, Kathrin Jäntsch, Marco Niello, Klaus Schicker, David Sulzer, Leticia González*, Nuno Maulide* and Harald H. Sitte*
    Fluorescent PyrAte-(S)-citalopram conjugates enable imaging of the serotonin transporter in living tissue
    Chemical Science 2025, 16, 6003–6013.
     
  • 209) Sabela Vega-Ces, Bogdan R. Brutiu, Daniel Kaiser and Nuno Maulide*
    Regioselective Synthesis of β,γ-Unsaturated Amides from Unactivated Alkenes
    The Journal of Organic Chemistry 2025, 90, 4121–4126.
     
  • 208) Nicolas G. Simonian, Bogdan R. Brutiu, Daniel Kaiser and Nuno Maulide*
    Cationic, Iodine(III)‐Mediated and Directed Diastereoselective Oxidation of Inert C–H Bonds in Cyclic Hydrocarbons
    Angewandte Chemie International Edition 2025, 64, e202421872.
     
  • 207) Iakovos Saridakis, Kish R. Adoni, Thomas Leischner, Bogdan R. Brutiu, Saad Shaaban, Giammarco Ferrari, Konstantinos Thalassinos* and Nuno Maulide*
    Rational Modification of a Cross-Linker for Improved Flexible Protein Structure Modeling
    Analytical Chemistry 2025, 97, 1273–1280.

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2024

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2023

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2022

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2021

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2020

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2019

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2018

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2017

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2016

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2015

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2014

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2013

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2012

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2011

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2010

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2009 and before

Postdoctoral Research (Prof. Barry M. Trost)

PhD Research (Prof. István E. Markó)

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Organic Syntheses Checking

1)      Preparation of a Z-Iodoalkene through Stork-Zhao-Wittig Olefination, Stereo-retentive Lithium-iodine Exchange and Z-Boronic acid Pinacol Ester Synthesis

Mathieu A. Morin, Samantha Rohe, Cecile Elgindy, and Michael S. Sherburn

Org. Synth. 2020, 97, 217-231.

Checked by Alexander Preinfalk, Martin Berger, and Nuno Maulide


2)      Palladium-Catalyzed Acetylation of Arylbromides

Milauni M. Mehta, Andrew V. Kelleghan, and Neil K. Garg

Org. Synth. 2021, 98, 68-83.

Checked by Martina Drescher, Daniel Kaiser, Nuno Maulide, Zach Ariki, Yuki Maekawa, and Cathleen Crudden


3)      Cu-catalyzed Allylic Perfluoroalkylation of Alkenes Using Perfluoro Acid Anhydrides: Preparation of N-(5,5,5-Trifluoro-2-penten-1-yl)phthalimide

Yuma Aoki, Shintaro Kawamura, and Mikiko Sodeoka

Org. Synth. 2021, 98, 84-96.

Checked by Martina Drescher, Daniel Kaiser, and Nuno Maulide


4)      Palladium-Catalyzed Hydrodefluorination of Fluoroarenes

Joseph J. Gair, Ronald L. Grey, Simon Giroux, and Michael A. Brodney

Org. Synth. 2021, 98, 131-146.

Checked by Vincent Porte, Daniel Kaiser, and Nuno Maulide


5)      Synthesis of the Isocyanide Building Block Asmic, anisylsulfanylmethylisocyanide

Embarek Alwedi, Bilal Altundas, Allen Chao, Zachary L. Ziminsky, Maanasa Natrayan, and Fraser F. Fleming

Org. Synth. 2021, 98, 147-170.

Checked by Anthony J. Fernandes, Martina Drescher, and Nuno Maulide


6)      Large-Scale Preparation of Oppolzer's Glycylsultam

Upendra Rathnayake, H. Ümit Kaniskan, Jieyu Hu, Christopher G. Parker, and Philip Garner

Org. Synth. 2021, 98, 463-490.

Checked by Bogdan R. Brutiu, Martina Drescher, Daniel Kaiser and Nuno Maulide


7)      Preparation of N-Formylamides by Oxidative Cleavage of N-Acylaminoacids

Nick Kilyeni

Org. Synth. 2022, 99, 29-37.

Checked by Miran Lemmerer, Manuel Schupp, and Nuno Maulide


8)      A Convenient Method for the Removal of Tetrabutylammonium Salts from Desilylation Reactions

Luca McDermott, Dominick C. Witkowski, and Neil K. Garg

Org. Synth. 2022, 99, 53-67.

Checked by Philipp Spieß, Daniel Kaiser and Nuno Maulide


9)      Synthesis of Phenols from Benzoic Acids

Wenzhang Xiong, Rui Wang, Zhengqiang Liu, Feng Peng, Ralph Zhao, and Wenbo H. Liu

Org. Synth. 2023, 100, 199-217.

Checked by Martina Drescher, Saad Shaaban and Nuno Maulide


10) Preparation of Pyrylium Tetrafluoroborate (Pyry-BF4)

Alejandro Gómez-Palomino, Clément Ghiazza, Julia Busch, Lucas Wagner and Josep Cornella

Org. Synth. 2023, 100, 361-381.

Checked by Thomas Leischner, Benjamin Thomas Jones, and Nuno Maulide


11) Preparation of 4-(5-(p-Tolyl)-3-(trifluoromethyl)-1H-pyrazol-1-yl)benzenesulfonyl fluoride (ArSO2F)

Lucas Wagner, Clément Ghiazza and Josep Cornella

Org. Synth. 2023, 100, 382-393.

Checked by Haoqi Zhang, Daniel Kaiser and Nuno Maulide


12) Synthesis of Deuterated 1H-Indole-3-carboxaldehyde via Catalytic Vilsmeier-Haack Reaction

Jing Xue, Yushan Zhang, Bing Zhong and Jin-Dong Yang

Org. Synth. 2024, 101, 21-33.

Checked by Paolo Piacentini, Omar Abdo and Nuno Maulide


13) Difluoromethylation of Phenols

Allison T. Hands, Zachary G. Walters, Jacob P. Sorrentino, and Neil K. Garg

Org. Synth. 2024, 101, 164-180.

Checked by Yi Xiao, Milos Vavrik and Nuno Maulide


14) Preparation of S-Methyl Methanethiosulfonate from Dimethyl Sulfoxide Initiated by Oxalyl Chloride

Xixuan Zhao, Shuai Peng, Hao Wang, Shuai Huang, Baoguo Sun, Hongyu Tian and Sen Liang

Org. Synth. 2024, 101, 395-409.

Checked by Roberto Tinelli, Sophie Woolford and Nuno Maulide


15) Synthesis of Borane-Ammonia and its Application in the Titanium Tetrachloride Catalyzed Reduction of Carboxylic Acids, Including N-Protected Amino Acids

Henry J. Hamann, Abdulkhaliq A. Alawaed, and P. Veeraraghavan Ramachandran

Org. Synth. 2025, 102, 19-44.

Checked by Gwyndaf A. Oliver, Konstantin Günther and Nuno Maulide


16) Preparation of 1,3-Dihydroxyphenazine

Trevor Dzwiniel, Emma Markun, James A. Kaduk, Aaron Hollas, Krzystof Pupek, and Nicholas Boaz

Org. Synth. 2025, 102, 45-63.

Checked by Uros Vezonik, Florian Doubek and Nuno Maulide


17) Large-Scale NaBr/Selectfluor Mediated Alcohol Oxidation: Conversion of (-)-Borneol into (-)-Camphor

Shyam Sathyamoorthi

Org. Synth. 2025, 102, 100-113.

Checked by Sergio Armentia Matheu, Saad Shaaban, and Nuno Maulide


18) Synthesis of gem-Difluoroalkenes through Ramberg-Bäcklund Reaction of Alkyltriflones

Motoo Ohtsuka, Yasuyo Tahara-Tezuka, Yuuki Maekawa, Cathleen M. Crudden, and Masakazu Nambo

Org. Synth. 2025, 102, 315-334.

Checked by Nikolaos Skoulikas, Lorenz Erlbacher and Nuno Maulide


19) Umpolung Synthesis of α-Bromo Secondary Amides from Unactivated Hydroxamates

Rui Wang, Hao Cao, and Wenbo H. Liu

Org. Synth. 2025, 102, 601-624.

Checked by Irmgard Tiefenbrunner, Angela Hofmeister and Nuno Maulide


20) Synthesis of Aryl Halides via a Safer Sandmeyer Reaction Protocol

Tim Schulte, Felix Waldbach, Tobias Ritter

Org. Synth. 2026, 103, 101-120.

Checking Authors Kunj Kapur, Daniya Aynetdinova, and Nuno Maulide


21) Copper-Mediated Oxidative Bromodifluoromethylation of Phenols: Preparation of Phenyl 4-(bromodifluoromethoxy) benzoate

Wen-Juan Yuan, Chao-Lai Tong, and Feng-Ling Qing

Org. Synth. 2026, 103, 192-204.

Checking Authors Uroš Vezonik, Sabela Vega-Ces, and Nuno Maulide


22) Preparation of 2-Iodoxybenzoic Acid (IBX)

Marianna C. Tonoyan, Aimee K. Long, and Neil K. Garg

Org. Synth. 2026, 103, 205-217.

Checking Authors: Milos Vavrik, Nikolaos Skoulikas, and Nuno Maulide


23) Photochemical Synthesis of Pyrroles from Furans and Amines

Jaehyun You, Donghyeon Kim, and Yoonsu Park

Org. Synth. 2026, 103, 283-300.

Checking Authors: Eléonore Tacke, Bjarne T. Schulz, and Nuno Maulide


24) IBX-Mediated Amine Oxidation

Abigail W. Wilson, Giulianna A. Miseo, Christina A. Rivera, and Neil K. Garg*

Org. Synth. 2026, 103, 407-422.

Checking Authors: Jakob Frey, Andreas Benedikt zur Bonsen, and Nuno Maulide*

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